Learning Outcomes
Practice on classical techniques of chemical analysis (preparation of standard solutions- volumetric analysis),as well as instrumental techniques(spectroscopy UV/VIS, atomic absorption spectroscopy, high performance liquid chromatography, gas chromatography,refractory).
Course Content (Syllabus)
Standard Solutions, Preparation and control. Volumetric analysis: Acid-Base Titration, Determination of the composition of a mixture NaOH/Na2CO3. Oxidation-Reduction Titration (Determination of Fe2+ with KMnO4). Complexometric Titration (Water hardness determination using EDTA). Spectrophotometry UV-Vis – Lambert-Beer Law-Absorption curves (Determination of Fe2+ with o-phenanthroline). Atomic Absorption Spectrometry with flame, Instrumentation, Applications. (Determination of calcite-dolomite mixture). Mineralogical identification of calcite-dolomite mixture using X rays. Ion chromatography – determination of Cl-, NO3-, SO42- in water samples. Gas chromatography (Determination of alkanes mixture). Refractometry (Determination of sugars in water samples).
Keywords
Volumetric analysis, instrumental chemical analysis, spectroscopy, atomic absorption spectroscopy, chromatography
Course Bibliography (Eudoxus)
1. ΑΝΑΛΥΤΙΚΗ ΧΗΜΕΙΑ (θέματα και προβληματα), Στυλιανός Λιοδάκης
2.ΕΝΟΡΓΑΝΗ ΧΗΜΙΚΗ ΑΝΑΛΥΣΗ, Ι.Παπαδογιάννης, Β.Σαμανίδου
3.ΠΟΣΟΤΙΚΗ ΧΗΜΙΚΗ ΑΝΑΛΥΣΗ ΤΟΜΟΣ Ι, , Daniel Harris ΙΔΡΥΜΑ ΤΕΧΝΟΛΟΓΙΑΣ & ΕΡΕΥΝΑΣ-ΠΑΝΕΠΙΣΤΗΜΙΑΚΕΣ ΕΚΔΟΣΕΙΣ ΚΡΗΤΗΣ 2009
4.ΕΝΟΡΓΑΝΗ ΑΝΑΛΥΣΗ ΘΕΜΙΣΤΟΚΛΗΣ Π. ΧΑΤΖΗΪΩΑΝΝΟΥ, ΜΙΧΑΗΛ Α. ΚΟΥΠΠΑΡΗΣ ΕΛΕΝΗ ΧΑΤΖΗΙΩΑΝΝΟΥ 1990