Learning Outcomes
Education on advanced techniques of chemical analysis, applications on the determination of chemical parameters of natural samples, evaluation of measurements, reference writing and its open presentation to the students of the course.
Course Content (Syllabus)
Theory:
Applications of statistics on chemical analysis
Random and systematic errors
Rejection of dubious values
Accuracy control
Comparison of experimental mean values
Determination of detection limit
statistically significant digits/
Organization of chemical laboratory/ collection and conservation of samples
Solubilization of solid samples
Separation techniques/ Extraction/ion exchange/
Chromatographic techniques: ion chromatography,gas chromatography
Atomic spectroscopy and graphite furnace(GFAA)/ ICP, FTIR, TG-DTA
Laboratory experiments:
-Determination of ionic constituents in atmospheric samples with ion chromatography
-Solubilization of environmental and biological samples and determination of metals with AAS (GRIPHITE FURNACE)
-Determination of Mercury with cold vapor technique
-Determination of total organic carbon (TOC) in potable water and wastes
-Identification of organic and inorganic compounds with FT-IR
-Qualitative and Quantitative determination of inorganic compounds with TG-DTA.
Keywords
Instrumental chemical analysis, advanced techniqhues, Chromatography, Spectroscopy.
Course Bibliography (Eudoxus)
Χημεία περιβάλλοντος Φυτιάνος Κωνσταντίνος Κ.,Σαμαρά - Κωνσταντίνου Κωνσταντινή UNIVERSITY STUDIO PRESS - ΑΝΩΝΥΜΟΣ ΕΤΑΙΡΙΑ ΓΡΑΦΙΚΩΝ ΤΕΧΝΩΝ ΚΑΙ ΕΚΔΟΣΕΩΝ 2009
Σ. Λιοδάκη, Αναλυτική Χημεία, Εκδόσεις ΠΑΠΑΣΩΤΗΡΙΟΥ, 2001.
Harris D.C., Ποσοτική χημική ανάλυση, Πανεπιστημιακές εκδόσεις Κρήτης, Ηράκλειο 2009.
Ι. Παππαδογιάννη, Εκδόσεις ΖΗΤΗ, Διαχωριστικές Τεχνικές στην Ενόργανη Χημική Ανάλυση, 1992.
Σημειώσεις: Μ. Μήτρακας, Εργαστηριακές Σημειώσεις Ατομικής Απορρόφησης και Εκπομπής, 2002.
Additional bibliography for study
L. Cleseri, A. Greenberg, R. Trusseli, Standard Methods for the Examination of Water and Wastewater, APHA, 1998.
J.C. Miller and J.N. Miller, Statistics for Analytical Chemistry, Ellis Horwood PTR Prentice Hall, 1993.
Mendham J., Denney R.C., Barnes J.D., Thomas M.J.K., “Vogel’s Quantitative Chemical Analysis”, 6th Ed. Prentice Hall (2000).
Harris D.C., Exploring Chemical Analysis, W.H. Freeman and Company, 1996.
Θ. Χατζηιωάννου – Μ. Κοππάρη, Ενόργανη Ανάλυση, 1997.