Separation Techniques in Chemical Analysis
| Title | ΜΕΘΟΔΟΙ ΔΙΑΧΩΡΙΣΜΟΥ ΣΤΗ ΧΗΜΙΚΗ ΑΝΑΛΥΣΗ / Separation Techniques in Chemical Analysis |
| Code | Κ203 |
| Faculty | Sciences |
| School | Chemistry |
| Cycle / Level | 1st / Undergraduate, 3rd / Doctorate |
| Teaching Period | Winter |
| Common | No |
| Status | Active |
| Course ID | 40002689 |
Programme of Study: PPS-Tmīma CΗīmeías (2016-sīmera)
Registered students: 36
| Orientation | Attendance Type | Semester | Year | ECTS |
|---|---|---|---|---|
| THEŌRĪTIKĪ CΗĪMEIA KAI CΗĪMIKĪ EKPAIDEUSĪ | Optional Courses | 7 | 4 | 5 |
| CΗĪMIKĪ ANALYSĪ-PERIVALLON-ĪLEKTROCΗĪMEIA | Elective Course belonging to the selected specialization (Elective Specialization Course) | 7 | 4 | 5 |
| CΗĪMIKĪ SYNTHESĪ-VIOCΗĪMEIA KAI VIOEFARMOGES | Optional Courses | 7 | 4 | 5 |
| CΗĪMIKĪ TECΗNOLOGIA KAI VIOMĪCΗANIKĪ CΗĪMEIA | Optional Courses | 7 | 4 | 5 |
| Academic Year | 2020 – 2021 |
| Class Period | Winter |
| Faculty Instructors |
|
| Weekly Hours | 4 |
| Class ID | 600170659
|
Course Type 2011-2015
Knowledge Deepening / Consolidation
Mode of Delivery
- Face to face
- Distance learning
Digital Course Content
- e-Study Guide https://qa.auth.gr/en/class/1/600170659
- eLearning (Moodle): https://elearning.auth.gr/course/view.php?id=11802
Erasmus
The course is also offered to exchange programme students.
Language of Instruction
- Greek (Instruction, Examination)
Learning Outcomes
The students can become familiar with the modern separation techniques, be informed upon current applications. They can also be familiar with analytical method development and troubleshooting.
General Competences
- Apply knowledge in practice
- Retrieve, analyse and synthesise data and information, with the use of necessary technologies
- Adapt to new situations
- Work autonomously
- Work in teams
Course Content (Syllabus)
Theoretical aspects of separation techniques. Sample preparation techniques. Preconcentration. Solid phase extraction. Supercritical fluid extraction. High Pressure Liquid Chromatography. Capillary electrophoresis. Ion chromatography. Gas chromatography. Hyphenated techniques GC-MS, LC-MS, preparative chromatography, chiral chromatography. Column switching techniques. Applications of separation techniques. Troubleshooting in HPLC. Principles, errors and interferences. Analytical method validation. Real sample analysis. Determination of caffeine, theobromine, theophylline, mefenamic acid, vitamins, paracetamol, in pharmaceuticals and biological samples, after solid phase extraction. Determination of inorganic ions by ion chromatography. Calculation of chromatographic parameters.
Keywords
Separation techniques, HPLC, GC, CE, Ion chromatography, Troubleshooting, Method validation
Educational Material Types
- Slide presentations
- Multimedia
- Book
Course Organization
| Activities | Workload | ECTS | Individual | Teamwork | Erasmus |
|---|---|---|---|---|---|
| Lectures | 26 | 1.0 | |||
| Laboratory Work | 20 | 0.8 | |||
| Reading Assigment | 66 | 2.6 | |||
| Written assigments | 10 | 0.4 | |||
| Exams | 3 | 0.1 | |||
| Total | 125 | 5 |
Student Assessment
Student Assessment methods
- Written Exam with Multiple Choice Questions (Formative, Summative)
- Written Exam with Short Answer Questions (Formative, Summative)
- Written Exam with Extended Answer Questions (Formative, Summative)
- Written Assignment (Formative, Summative)
- Oral Exams (Formative, Summative)
- Written Exam with Problem Solving (Formative, Summative)
- Labortatory Assignment (Formative, Summative)
Bibliography
Course Bibliography (Eudoxus)
ΣΥΓΧΡΟΝΕΣ ΔΙΑΧΩΡΙΣΤΙΚΕΣ ΤΕΧΝΙΚΕΣ ΣΤΗΝ ΕΝΟΡΓΑΝΗ ΧΗΜΙΚΗ ΑΝΑΛΥΣΗ. Ι.ΠΑΠΑΔΟΓΙΑΝΝΗΣ
Additional bibliography for study
επιλεγμένες εργασίες
Last Update
05-03-2021
